高压反应釜
- 网络Autoclave;High pressure reactor;high-pressure reactor
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在高压反应釜中采用Mn-Ce和Co-Bi复合催化剂通过催化湿式氧化法处理丙烯腈废水。
Catalytic wet air oxidation ( CWAO ) of wastewater from acrylonitrile production over complex oxides catalysts of Mn-Ce and Co-Bi was investigated in a high pressure reactor .
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在微型高压反应釜中(120ml),考察了酸催化三聚甲醛和甲酸甲酯制备羟基乙酸甲酯的偶联反应,并对酸催化剂中H+的作用进行了研究。
Acid catalyst and H + catalysis in the acid catalysts were studied for synthesis of methyl glycolate via coupling of methyl formate and trioxane in a microform high-pressure autoclave ( 120mL ) .
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在高压反应釜中考察了反应温度、催化剂、pH、物料配比及搅拌速率对反应结果的影响。
The effect of different factors on the hydrolysis reaction , such as reaction temperature , catalyst , pH and stirring rate was investigated at high pressure .
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用高压反应釜对一种骨架Ni催化剂和八种Pd/Al2O3催化剂在苯乙烯环境下,对连串反应苯乙炔的选择性加氢性能进行了实验评价。
The catalytic performance of a Raney nickel catalyst and eight Pd / Al_2O_3 catalysts in selective hydrogenation of phenylacetylene in the presence of styrene was studied using a high-pressure reactor .
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通过对几种还原剂和还原方式的探索,得到最优化的的还原方式及具体还原参数:高压反应釜乙二醇160℃还原,PH值为11。
The most optimal way and the specific parameters of reduction are obtained by means of several explorations to the reductions . Ethylene glycol is acted as reducing agent in autoclave ( 160 ℃) and PH is 11 .
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利用高温高压反应釜研究油田常用的四种S135钢在含CO2聚合物钻井液中腐蚀行为。
Corrosion behavior of four kinds of S135 steel in polymer drilling fluids containing CO2 is investigated using high temperature high pressure autoclave .
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在130℃,以三氯化铁(Fe2O3·6H2O)和乌洛托品((CH2)6N4)为基本原料在高压反应釜(聚四氟乙烯内衬)中进行反应。
At 130 ℃, the reaction was carried out in a sealed Teflon-lined autoclave employed Urotropine (( CH_2 ) _6N_4 ) and ferric chloride ( Fe_2O_3 ? 6H_2O ) as the reactants .
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以碱性化合物K2CO3、Ca(OH)2以及Ru/C为催化剂,在间歇式高压反应釜中,对半纤维素在超临界水中的气化制氢特性进行了实验研究。
The gasification of hemicellulose in supercritical water to produce hydrogen-rich gas was performed , and K_2CO_3 , Ca ( OH ) _2 and Ru / C were used as catalysts during the gasification processes .
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采用高压反应釜研究了无机铵盐添加剂对Rh催化的高碳烯烃(C8、C12烯烃)氢甲酰化反应的影响。
The influence of inorganic ammonium salts on rhodium-catalyzed hydroformylation of higher olefins ( C 8 and C 12 olefins ) was investigated with an autoclave .
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在250mL不锈钢高压反应釜中,以TS1分子筛为催化剂,丁酮、氨水和过氧化氢进行氨氧化合成丁酮肟。
Butanone oxime was prepared from butanone , ammonia and H_2O_2 by ammoxidation with catalyst of titanium silicalite-1 ( TS-1 ) in 250 mL stainless autoclave .
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本文以泡桐为原料以水为溶剂,在1L间歇式高压反应釜中进行直接液化实验,通过预试验设计对反应温度、停留时间和液料比进行了考察。
Paulownia direct liquefaction is processed in a 1L batch autoclave with water as a solvent . And the reaction temperature , residence time and liquid ratio are investigated by the pre-experiment design .
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在高压反应釜中,对苯二甲酸二甲酯经两步催化加氢反应合成了1,4-环己烷:二甲醇。
The synthesis of1,4-cyclohexanedimethanol from dimethyl terephthalate by two-stage liquid-phase hydrogenation was studied .
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容错控制在浓硝酸高压反应釜中的应用研究
Fault-tolerant Control in the Application Research of The Continuous worked Strong nitric acid Autoclave
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本文通过结合现有高压反应釜的特点,重新设计制作了一个小型多腔发泡模具。
This paper according to the characteristics of the highpressure reaction kettle , designing a small porous foaming mold .
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一步水热法是将氧氯化锆和氨水按比例混和后,直接加入高压反应釜中进行水热反应的工艺。
ZnO green phosphor preparation process by the thermal oxidation of zinc sulfide with zirconium oxychloride as additive is investigated .
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在高压反应釜中对吸附饱和的活性炭进行多相催化湿式氧化,使活性炭得以再生,并氧化分解被脱附析出的有机物。
In a batch autoclave reactor , saturated adsorbent was regenerated in heterogeneous catalytic wet oxidation , and organic chemicals were oxidized and decomposed .
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最后,本文还对乙基咔唑吸氢和脱氢反应一体化过程进行研究,并在高压反应釜中对该过程进行循环实验。
Finally , hydrogenation-dehydrogenation integration process was studied , and the cyclic of this integrated process was followed , which were taken in a batch reactor .
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本实用新型的高压反应釜特别适用于具有较强的酸碱性化工原料的加工生产。
The high-pressure reaction kettle of the utility model is especially suitable for the processing and production of chemical raw materials with strong acidity and basicity .
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本论文主要考虑发泡压力,发泡温度,释压速率(或释压时间)和溶剂配比对气泡密度和气泡平均孔径的影响,并分别在高压反应釜中进行了实验,得出了各自的变化关系。
This paper mainly studied the effects of initial pressure , foaming temperature , depressurization rate , and solvent proportion on bubble density and average bubble size .
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对核心设备高压反应釜进行了选型,计算了壁厚,釜盖厚度,螺栓,搅拌轴,搅拌桨等。
The model of the core equipment-high pressure reactor is selected and the wall thickness , kettle cover thickness , bolts , stirring shaft , impeller , etc are calculated .
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采用浸渍法制备了Pt/活性碳毡催化剂,并在自制的高压反应釜上考察了该催化剂对四氯化碳加氢制氯仿反应的性能。
Pt / active carbon fiber catalyst was prepared by an impregnation method , and its performance for transforming carbon tetrachloride to chloroform was investigated in a high pressure static reactor .
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在小型高压反应釜中研究了铑系催化剂对于α,ω-二元羧酸单酯加氢生成ω-羟基羧酸酯的催化性能。
The catalytic performance of rhodium based bicomponent catalysts in the hydrogenation of α,ω - dicarboxylic acid monoesters to ω - hydroxy carboxylic acid esters was investigated by using a portable autoclave .
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以己二腈加氢制己二胺为探针反应物,采用高压反应釜进行间歇反应评价和磁稳定床连续加氢装置评价。
The evaluation of the catalysts was carried on an autoclave and a continuous hydrogenation unit with a magnetic stabilized bed ( MSB ) reactor , and adiponitrile was used as a probe reactant .
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以烷基酚、甲醛、环氧乙烷和环氧丙烷为原料,合成海洋原油用破乳剂。破乳剂的合成主要是通过高压反应釜将起始剂与环氧乙烷、环氧丙烷共聚得到。
The demulsifier is synthesized by using alkylphenol , formaldehyde , ethylene oxide and propylene oxide . Demulsifiers are synthesized mainly by co-polymerizing with ethylene oxide , propylene oxide and acceptor in high-pressure kettle .
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采用质量分数为50%的工业双氧水为引发剂,乙醇为溶剂,丁二烯为单体,在不锈钢高压反应釜中进行自由基溶液聚合,合成了液体端羟基聚丁二烯。
The hydroxyl terminated polybutadiene ( HTPB ) was synthesized by free radical polymerization in higher pressure reactor , with H 2O 2 ( 50 % by weight ) as initiator , alcohol as solvent .
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按照一定的配比,将氯化铟和间苯二酚完全溶解于甲酰胺的水溶液中,然后转入聚四氟乙烯高压反应釜中,密封后在160℃下水热反应一定时间,即得到氢氧化铟中空球。
With a suit ratio , Indium trichloride and resorcinol dissolve absolutely into the solution of formamide water solution . The reactants were transformed into 22 ml teflon-sealed autoclave and heated at 160 ℃ for some hours .
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为了解不同介质中天然气水合物的声学特性,在特制的高压反应釜中分别进行了纯水、松散沉积物和岩心中甲烷水合物的生成和分解的模拟实验,同时应用超声技术进行了探测。
To understand the acoustic characteristics of gas hydrates in different media , the ultrasonic detecting technology is applied to the experimental study of gas hydrates in the pure water , the unsolidified sediment , and the core sample , respectively .
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本论文采用高压反应釜中的催化/还原热解法合成了片状、蜂窝状、以及竹节状的碳材料,探讨了产物的形成过程,并初步研究了材料在染料吸附、电化学储锂方面的性能。
In this dissertation , carbon materials with sheet-like , honeycomb-like , and bamboo-shaped architectures were prepared via catalytic or reduction pyrolysis routes in stainless-steel autoclave . The growth process of products was investigated , and the properties including adsorption activity and Li + storage were also studied .
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在2L高压间歇反应釜中,以高浓度难降解乳化废水为处理对象,研究了温度对铜盐均相湿式氧化的影响和动力学特征。
Catalytic wet air oxidation of high-strength refractory emulsification wastewater was performed in a 2L high-pressure batch autoclave , with emphasis on influence and dynamics characteristic of temperature to homogenous catalytic wet air oxidation of Cu salts .
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超高压聚乙烯反应釜
Super high pressure polyethylene reaction pot