薄层层析硅胶
薄层层析硅胶-
方法：用硅胶柱层析法对平贝总碱进行分离纯化，固定相为薄层层析硅胶G，流动相为乙酸乙酯-甲醇-氨水（17：2：1）。
The solid phase was thin layer chromatography silica gel G and the mobile phase was ethyl acetate-methanol-ammonia ( 17:2:1 ) .
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薄层层析硅胶GF254为固定相，乙酸乙酯甲醇水（7-2-1，v/v/v）为展开剂，熊果苷和氢醌的Rf值分别为0.56和0.67。
The optimal conditions of TLC were as follows : silica gel GF254 as stationary phase , ethyl actate-methanol-water ( 7-2-1 , v / v / v ) as mobile phase .